Solid State NMR Spectroscopy for Biopolymers: Principles and Applications (Hardcover)

Part I Principles 1. Introduction 2. Solid state NMR approach 2.1. CP-MAS and DD-MAS NMR 2.2. Quadrupolar nuclei 3. Brief outline of NMR parameters 3.1. Chemical shifts 3.2. Relaxation parameters 3.3. Dynamics-dependent suppression of peaks 4. Multinuclear approaches 4.1. 31P NMR 4.2. 2H NMR 4.3. 17O NMR 5. Experimental strategies 5.1. Isotope enrichment (labeling) 5.2. Assignment of peaks 5.3. Ultra high-field and ultra high-speed MAS NMR spectroscopy 6. NMR constraints for structural determination 6.1. Orientational constraint 6.2. Interatomic distance 6.3. Torsion angles 6.4. Conformation-dependent 13C chemical shifts 7. Dynamics 7.1. Fast motions with motional frequency 106 Hz 7.2. Intermediate or slow motions with frequency between 106 and 103 Hz 7.3. Very slow motions with frequency