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· 분류 : 외국도서 > 과학/수학/생태 > 과학 > 화학 > 분석화학
· ISBN : 9780124115897
· 쪽수 : 534쪽
· 출판일 : 2015-09-04
목차
The Basics of Modern NMR Spectroscopy: What is NMR? Instrumentation. Creating NMR Signals.
Spin-Echo and Polarization Transfer: Spin-Echo Formation in Homonuclear and Heteronuclear Systems. Cross-Polarization. Polarization Transfer in Reverse.
The Second Dimension: Data Acquisition in 2D NMR. Data Processing in 2D NMR. Plotting 2D Spectra.
Nuclear Overhauser Effect: nOe and Selective Population Transfer. Relaxation. Mechanism of nOe. Factors Affecting nOe. Some Practical Hints.
Important 2D NMR Experiments: Homo- and Heteronuclear J-Resolved Spectroscopy. Homonuclear and Heteronuclear Shift-Correlation Spectroscopy. Two-Dimensional Nuclear Overhauser Spectroscopy. Two-Dimensional Chemical Exchange Spectroscopy. Homonuclear Hartmann-Hahn Spectroscopy (HOHAHA), or Total Correlation Spectroscopy (TOCSY). Inverse NMR Spectroscopy. Inadequate.
The Third Dimension: Basic Philosophy. Types and Positions of Peaks in 3D Spectra.
Recent Developments in NMR Spectroscopy: Selective Pulses in Modern NMR Spectroscopy. One-Dimensional Experiments Using Soft Pulses. Heteronuclear Selective 1D NMR Experiments. Two-Dimensional Experiments Using Soft Pulses. Soft Excitation in Two Dimensions. Three-Dimensional Experiments Using Soft Pulses. Field Gradients.
Logical Protocol for Solving Complex Structural Problems: 3-Hydroxylupanine. (1). (+)-Buxalongifolamidine. (2). References. Subject Index.
