[eBook Code] Inorganic Syntheses, Volume 22 (eBook Code, 1st)

Chapter One SOLID STATE.

1. Ternary Chlorides and Bromides of the Rare Earth Elements.

2. Quaternary Chlorides and Bromides of the Rare Earth Elements: Elpasolites A¹₂B¹RE¹¹¹X₆ (r(A¹) > r(B¹)).

3. Tantalum as a High-Temperature Container Material for Reduced Halides. 

4. Cesium Scandium(II) Trichloride.

5. Zirconium Monochloride and Monobromide.

6. Lanthanum Triiodide (And Other Rare Earth Metal Triiodides).

7. Lanthanum Diiodide.

8. Trichlorides of Rare Earth Elements, Yttrium, and Scandium.

9. Single Crystal Growth of Oxides by Skull Melting: The Case of Magnetite (Fe3O4).

10. Lithium Nitride, Li3N.

11. The Alkali Ternary Oxides A_xCoO₂ and A_xCrO₂ (A = Na, K).

12. Zeolite Molecular Sieves.

13. Lead Ruthenium Oxide, Pb₂ [Ru_2-xPb⁴⁺_x]O_6.5.

14. Calcium Manganese Oxide, Ca₂Mn₃O₈.

15. Synthesis of Silver Tetratungstate.

16. Cadmium Mixed Chalcogenides and Layers of Cadmium (Mixed) Chalcogenides on Metallic Substrates.

17. Layered Intercalation Compounds.

18. Iron Titanium Hydride (FeTiH_1.94).

19. Aluminum Lanthanum Nickel Hydride.

Chapter Two TRANSITION METAL COMPLEXES AND COMPOUNDS.

20. Purification of Copper(I) Iodide.

21. Cobalt(III) Amine Complexes with Coordinated Trifluoromethanesulfonate.

22. 2,9-Dimethyl -3,10-diphenyl-l,4,8,11 -tetraazacyclotetradeca -1,3,8,10-tetraene, (Me₂Ph₂ [14]-1,3,8,10 -tetraeneN₄) Complexes.

23 Dichlorobis(3,3',3" -phosphinidynetripropionitrile) nickel(II) and Dibromobis (3,3',3" -phosphinidynetripropionitrile) nickel(II) Monomers and Polymers.

24. Polymer-stabilized Divanadium.

25. Triamminechloroplatinum(II) Chloride.

26. Chlorotris(dimethylsulfide)platinum(II) Compounds.

27. Tetrabutylammonium Trichloro (dimethylsulfide) platinum(II).

Chapter Three MAIN GROUP, LANTHANIDE, ACTINIDE, AND ALKALI METAL COMPOUNDS.

28. Tributyl Phosphorotrithioite (C₄H₃S)₃P from Elemental Phosphorus.

29. Preparation of Dimethylphenylphosphine.

30. Electrochemical Synthesis of Salts of Hexahalodigallate (II) and Tetrahalogallate(III) Anions.

31. Polymeric Sulfur Nitride (Polythiazyl), (SN_x).

32. Pyridinium Hexachloroplumbate(IV).

33. Bis[(4,7,13,16,21,24 -hexaoxa -l,l0 -diazabicyclo[8.8.8.] hexacosane) potassium] Tetrabismuth (2-).

34. [5,10,15,20-Tetraphenylporphyrinato(2-l)] Lanthanides and Some [5,10,15,20-Tetraphenylporphyrinato(2-l)] Actinides.

35. [μ-Nitrido-bis(triphenylphosphorus)] (1+) Tricarbonylnitrosylferrate (1-) and [μ-Nitrido-bis (triphenylphosphorus)] (1+) Decacarbonyl-μ-nitrosyl-triruthenat(1-), [(Ph₃P)₂N] [Fe(CO)₃(NO)] and [(Ph₃P)₂N] [Ru₃(CO)₁₀(NO)].

36. Metallacyclopentane Derivatives of Palladium.

37. Metallacyclopentane Derivatives of Cobalt, Rhodium, and Iridium.

38. Cycloolefin Complexes of Ruthenium.

39. Mononuclear Pentacarbonyl Hydrides of Chromium, Molybdenum, and Tungsten.

Chapter Five COMPOUNDS OF BORON.

40. [(2,2-Dimethylpropanoyl) oxy] diethylborane, ((Pivaloyloxy) diethylborane).

41. Tetraethyldiboroxane.

42. Diethylmethoxyborane, (Methyl diethylborinate).

43. Diethylhydroxyborane, (Diethylborinic acid).

44. Bis [μ-(2,2-dimethylpropanoato-O, O)]-diethyl-μ-oxo-diboron.

45. Alkali Metal (Cyclooctane-l,5-diyl) dihydroborates(1-).

46. Decaborane(14).

47. Dichlorophenylborane.

48. (Dimethy1amino)diethylborane.

49. 2,3-Diethyl-2,3-dicarba-nido-hexaborane(8).

50. 2, 2',3, 3'-Tetraethyl-1,1-dihydro- [1,1'-commo-bis(2,3-dicarba-1-ferra-closo-heptaborane)] (12), [2,3-(C₂H₅)₂C₂B₄H₄]₂ FeHz₂, and 2,3,7,8-Tetraethyl-2,3,7,8 -tetracarbadodecaborane(12), (C₂H₅)₄C₄B₈H₈.

51. [¹⁰B]-Labeled Boron Compounds.

52. The Thiadecaboranes arachno- [6-SB₉H₁₂]^-, nido-6-SB₉H₁₁, and closo-1-SB₉H₉.

53. Potassium Dodecahydro-7-8 -dicarba-nido-undecabora(1-), K[7,8-C₂B₉H₁₂], Intermediates, Stock Solution, and Anhydrous Salt.

54. 3-(η⁵-Cyclopentadienyl) -1,2-dicarba-3-cobalta -closo-dodecaborane(11), 3-(η⁵-C₅H₅)-3-Co-1, 2-C₂B₉H₁₁.

55. 2,6-Dicarba-nido-nonaborane(11), 2, 6-C₂B₇H₁₁.

56. 9-(Dimethyl sulfide)-7,8 -dicarba-nido-undecaborane(11), 9-[(CH₃)₂S]-7,8-C₂B₉H₁₁.

57. Direct Sulfhydrylation of Boranes and Heteroboranes, 1,2, -Dicarba-closo-dodecaborane(12) -9-thiol, 9-HS-1, 2-C₂B₁₀H₁₁.

Index of Contributors.

Subject Index.

Formula Index.