Polymer Characterization : Physical Techniques, 2nd Edition (Paperback, 2 ed)

· 제목 : Polymer Characterization : Physical Techniques, 2nd Edition (Paperback, 2 ed) 
· 분류 : 외국도서 > 과학/수학/생태 > 과학 > 화학 > 화학 일반
· ISBN : 9780748740055
· 쪽수 : 481쪽
· 출판일 : 2000-09-28

INTRODUCTION: PRELIMINARY SURVEY

The Purpose of Characterization
Molecular Architecture
Amorphous Polymers
Crystallizing Polymers
Survey of Characterization Techniques
References
Further Reading

MOLECULAR MASS DETERMINATION

Introduction
Primary Methods
Secondary Methods
Other Methods
Conclusions
Further Reading
Exercises
INTRODUCTION TO SPECTROSCOPIC TECHNIQUES
General Remarks
Strategy in Spectroscopic Studies
Energy Level Calculations
Properties of Electromagnetic Radiation
Double Beam Optics
Fourier Transform Spectroscopy
References

ULTRAVIOLET-VISIBLE SPECTROSCOPY

Introduction
Instrumentation
Theoretical Estimation of Electronic Energy Levels
Application to Polymers
References
VIBRATIONAL SPECTROSCOPY: INFRARED AND RAMAN SPECTROSCOPY
Fundamentals of Vibrational Spectroscopy
Experimental Techniques
Applications to Polymers
Raman Analysis
Near-Infrared (NIR)
Conclusions
References
NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY
Introduction
Principles of Magnetic Resonance
Experimental Techniques
Applications of NMR to Polymers
NMR of Polymers in the Solid State
Two-Dimensional NMR
NMR Imaging
Conclusions
References
Exercises

ELECTRON SPIN RESONANCE SPECTROSCOPY

Introduction
Basic Theory
Experimental Considerations
Polymerization Studies
Radiation Effects in Polymers
Mechanical Degradation
Thermal Degradation
Relaxation Studies
ESR Imaging
Conclusions
Further Reading
Exercises

XRAY DIFFRACTION

Introduction
Generation and Properties of X-rays
Diffraction Theory
Practical Aspects
Applications to Polymer Characterization
Conclusions
References
Further Reading
Exercises
TRANSMISSION ELECTRON MICROSCOPY AND DIFFRACTION
Introduction
Layout of the TEM
Resolution Limitation
Electron Diffraction
Image Contrast
Operating Conditions and Procedures for Beam-sensitive Materials
Polymer Studies in TEM
Multiple Dark Field Imaging
Scanning Transmission Electron Microscopy (STEM)
References
Further Reading
Exercises

SCANNING ELECTRON MICROSCOPY

Introduction
Design and Operation of the SEM
Observation of Polymers in the SEM
Examples of SEM Applications with Polymers
Conclusions
Further Reading
Exercises

LIGHT OPTICAL TECHNIQUES

Introduction
Refractive Index
Birefringence
Light Microscopy
Small Angle Light Scattering
References
Further Reading
Advanced Reading
Exercises

THERMAL ANALYSIS

Introduction
Differential Thermal Analysis (DTA) and Differential Scanning Calorimetry (DSC)
Thermomechanical Analysis
Thermogravimetric Analysis
Dynamic Mechanical Thermal Analysis
Dielectric Thermal Analysis (DETA)
References
DENSITY, SURFACE PROPERTIES AND NEUTRON DIFFRACTION
Density
Surface Analysis of Polymeric Materials
Chemical Analysis of the Polymer Surface
Surface Probe or Scanning Tip Microscopy
Neutron Scattering Studies
References
Further Reading
Exercises

MULTIPLE CHARACTERIZATION APPLICATIONS

The Structure of a Spherulite
Skin-core Characterization in Moulded Polymers
Weathering of Polymers
Particular Studies
Conclusions
References
THEORETICAL PREDICTIONS OF THE PHYSICAL PROPERTIES OF POLYMERIC MATERIALS
Introduction
Types of Approach Available for Modelling Polymer Physical Properties
Molecular Based Structural Additivity Calculations
Ab initio Calculations of Polymeric Properties
References
APPENDIX
INDEX