NMR and Chemistry : An introduction to modern NMR spectroscopy, Fourth Edition (Paperback, 4 ed)

THE THEORY OF NUCLEAR MAGNETIZATION
The Properties of the Nucleus of an Atom
The Nucleus in a Magnetic Field
The Source of the NMR Signal
A Basic NMR Spetrometer
Questions

THE MAGNETIC FIELD AT THE NUCLEUS: NUCLEAR SCREENING THE CHEMICAL SHIFT
Effects Due to the Molecule
Isotope Effects
Effects Due to Unpaired Electrons
The Chemical Shift
Note on Sample Preparation, Standardization, and Solvent and Temperature Effects
Questions

INTERNUCLEAR SPIN-SPIN COUPLING
The Mutual Effects of Nuclear Magnets on Resonance Positions
The Appearance of Multiplets Arising form Spin-Spin Coupling
Spin-Spin Coupling Satellites
The Description of Spin Systems
Second-Order Effects
Questions

NUCLEAR MAGNETIC RELAXATION
Relaxation Processes in Assemblies of Nuclear Spins
Dipole-Dipole Relaxation
Quardrupolar Relaxation
Spin Rotation Relaxation: Detailed Molecular Motion
Chemical Shift Anisotropy Relaxation
Scalar Relaxation
Examples of 13C Relaxation Times
Questions

THE SPECTROMETER
The Magnet and Field Homogeneity
The Probe
Field-Frequency Lock
The Transmitter
The Detection System
Production of the Spectrum
Rapid Multiple Pulsing
Manipulations of Collected Data
Questions

MAKING THE SPINS DANCE
Decoupling
Composite Pulses
Refocusing Pulse
Questions

NMR SPECTRA OF EXCHANGING AND REACTING SYSTEMS
Systems at Equilibrium
Reaction Monitoring of Systems not at Equilibrium
Questions

MULTIPLE RESONANCE AND ONE-DIMENSIONAL PULSE SEQUENCES
Decoupling Difference Spectroscopy
The Nuclear Overhauser Effect
One-Dimensional Mutliphase Sequences
Exercises in Spectral Interpretation

TWO-DIMENSIONAL NMR SPECTROSCOPY
J-Resolved Two-Dimensional NMR Spectroscopy
Homonuclear COSY NMR Spectroscopy
Heteronuclear COSY NMR Spectroscopy
HOHAHA or TOCSY
Two-Dimensional INADEQUATE
Overhauser and Magnetization Transfer Based Two-Dimensional NMR Spectroscopy
Inverse Detection
Three-Dimensional NMR Spectroscopy
Questions

MAGNETIC RESONANCE IMAGING AND BIOMEDICAL NMR
Producing an Image
Whole Body Imaging
Diffusion and Flow
Chemical Shift Imaging
Biological Uses of Imaging - Imaging Microscopy
Industrial Uses of Imaging Techniques
Biomedical NMR

HIGH-RESOLUTION SOLID-STATE NMR
Magic Angle Spinning
Spin-1/2 Nuclei with Low Magnetogyric Ratios
I=1/2 Nuclei with High Magnetogyric Ratios
MAS of Quadropolar Nuclei
Some Applications
Deuterium, An Integral-Spin Nucleus
Questions

Bibliography
Answers to Questions
Index